3-Ethoxy-4-methoxybenzaldehyde → alpha-(3-Ethoxy-4-methoxyphenyl)-N-n-butylnitrone

HRID 2305792

反応式

HRID 2305792 の反応式
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH:7]=O)[CH3:2].[CH2:14]([NH:18][OH:19])[CH2:15][CH2:16][CH3:17]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:7]=[N+:18]([CH2:14][CH2:15][CH2:16][CH3:17])[O-:19])[CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[CH3:2]

参加物

3

反応物 2

HCID 2447283-Ethoxy-4-methoxybenzaldehydeHCID 10034579N-Hydroxy-1-butanamine

生成物 1

HCID 86587899alpha-(3-Ethoxy-4-methoxyphenyl)-N-n-butylnitrone

実験手順

The title compound was prepared according to the procedures described in Examples 11 using 3-ethoxy-4-methoxybenzaldehyde and N-n-butylhydroxylamine. The title compound was isolated in 41.1% yield as a solid, m.p. 117.3° C.

後処理

  1. customThe title compound was prepared

出典と根拠

ORDレコード
ord-6d502486f28244beb1261b2fce624a16
出典データセット
uspto-grants-2002_08
特許番号
US06441032B1

関連ノート

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