2-Methoxybenzaldehyde → alpha-(2-methoxyphenyl)-N-t-butylnitrone

HRID 2305812ノート

反応式

HRID 2305812 の反応式
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=O.[C:11]([NH:15][OH:16])([CH3:14])([CH3:13])[CH3:12]>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=[N+:15]([C:11]([CH3:14])([CH3:13])[CH3:12])[O-:16]

参加物

3

反応物 2

HCID 86582-MethoxybenzaldehydeHCID 98586N-tert-butylhydroxylamine

生成物 1

HCID 85447185alpha-(2-methoxyphenyl)-N-t-butylnitrone

実験手順

The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1° C. (Rf=0.53 on a silica gel plate using ethyl acetate as the eluant).

後処理

  1. customThe title compound was prepared

出典と根拠

ORDレコード
ord-278ef9eefb9741c5bf9582b4aedf707c
出典データセット
uspto-grants-2002_08
特許番号
US06441032B1

反応ノート

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