化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl (4-iodophenyl)acetate → Ethyl (3'-hydroxybiphenyl-4-yl)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl (4-iodophenyl)acetate | HCID 14974990 | — |
| 反応物 | (3-(Methoxymethoxy)phenyl)boronic acid | HCID 22606941 | — |
| 生成物 | Ethyl (3'-hydroxybiphenyl-4-yl)acetate | HCID 25139319 | — |
反応手順
In a manner similar to that of Example 1(h), by reaction of 543 mg (3.6 mmol) of 3-methoxymethoxyphenylboronic acid with 700 mg (2.4 mmol) of ethyl 4-iodophenylacetate, 630 mg (68%) of the expected ethyl ester are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06831106B1 |
| 出典データセット | uspto-grants-2004_12 |
| ORD ID | ord-7f158b0390ca489a88f2fcd39fa54b93 |
| 出典メモ | uspto-grants-2004_12 |