反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH:7]([OH:10])[CH2:8][CH3:9])[S:5][CH:6]=1>ClCCl.[O-2].[O-2].[Mn+4]>[Br:1][C:2]1[CH:3]=[C:4]([C:7](=[O:10])[CH2:8][CH3:9])[S:5][CH:6]=1参加物
4
実験手順
11.5 g (52 mmol) of 1-(4-bromo-2-thiophenyl)-1-propanol are dissolved in 300 mL of dichloromethane. 60 g (690 mmol) of manganese dioxide are added and the reaction medium is stirred for 14 hours and then filtered. The desired product is obtained in the form of an orange-coloured oil (m=11.4 g; Y=99%).
後処理
- filtrationfiltered
出典と根拠
- ORDレコード
- ord-63d3a1ebd9e74ddabe581e351eae2e72
- 出典データセット
- uspto-grants-2004_12
- 特許番号
- US06831106B1
関連ノート
読み込み中…