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3,5-Difluorophenylacetic acid → N-[(3,5-difluorophenyl)acetyl]alanine iso-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| 反応物 | 2-methylpropyl (2S)-2-aminopropanoate | HCID 13743556 | — |
| 生成物 | N-[(3,5-difluorophenyl)acetyl]alanine iso-butyl ester | HCID 22894975 | — |
反応手順
Following General Procedure BI above, and using 3,5-difluorophenylacetic acid (Aldrich) and alanine iso-butyl ester (prepared following General Procedure BJ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06849650B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-bc8e9df341a24c0b9a70df7572a69ea5 |
| 出典メモ | uspto-grants-2005_02 |