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HRID 23114作成日：2026年10月26日

Cyclohexaneacetic acid → N-(cyclohexyIacetyl)-L-alanine iso-butyl ester

https://huagongshe.com/reaction/23114

反応式

関与物質

役割名称HCID仕込み量
反応物Cyclohexaneacetic acidHCID 21363—
反応物2-Methylpropyl (2S)-2-aminopropanoate hydrochlorideHCID 86584981—
生成物N-(cyclohexyIacetyl)-L-alanine iso-butyl esterHCID 54223838—

反応手順

Following General Procedure BB above, and using cyclohexylacetic acid (Aldrich) and L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as a solid having a melting point of 92° C.-93° C. The reaction was monitored by tlc on silica gel (Rf=0.39 in 1:3 EtOAc:hexane) and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06849650B2
出典データセットuspto-grants-2005_02
ORD IDord-8987fd35e1c749fda905895504669c82
出典メモuspto-grants-2005_02