化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 9,10-Dihydroanthracene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Anthracene | HCID 8418 | — |
| 反応物 | Cerium | HCID 23974 | — |
| 溶媒 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | 9,10-Dihydroanthracene | HCID 11940 | 59% |
反応手順
1.14 mmole of anthracene is reacted with 4.57 m atoms of cerium as powder in 7.5 ml of DME in the conditions of example 9 with application of ultrasound, thus producing anthracenecerium. After action of a methanol excess and the usual treatment, 9,10-dihydroanthracene was isolated with a yield of 59%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04845201 |
| 出典データセット | uspto-grants-1989_07 |
| ORD ID | ord-4d94dcbf8d314500877ef0fa80aacbef |
| 出典メモ | uspto-grants-1989_07 |