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Lead diacetate → Lead naphthenates
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lead diacetate | HCID 9317 | — |
| 反応物 | Potassium naphthalate | HCID 23664128 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Lead naphthenates | HCID 25021832 | — |
反応手順
On the other hand, 38 g of stannous chloride, 26 g of lead acetate and 200 g of water were charged into a 500 ml beaker equipped with a stirrer and the metal salts were dissolved into the water with stirring. This aqueous solution of the metal salts was added to the aforesaid aqueous solution of potassium naphthenate and a double decomposition reaction was then carried out for 1 hour at 30° C. The reaction mixture was dehydrated, dried and then extracted with toluene. The residue was heated under a reduced pressure of 10 mm Hg to distill off the toluene whereby stannous and lead naphthenates were obtained which had a tin content of 13.2% by weight and a lead content of 9.2% by weight.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04851153 |
| 出典データセット | uspto-grants-1989_07 |
| ORD ID | ord-6a1195b158f941739e297dc0d160e7e6 |
| 出典メモ | uspto-grants-1989_07 |