関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanethiol | HCID 6343 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 2-(7-Chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359142 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 2-(7-Chloro-6-ethylthioquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359231 | — |
反応手順
0.37 ml of ethyl mercaptan and 1.12 g of potassium carbonate were added to 2.0 g of 2-(7-chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine dissolved in 80 ml of dimethylformamide and the mixture was stirred at 90° C. for 4 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05591752 |
|---|
| 出典データセット | uspto-grants-1997_01 |
|---|
| ORD ID | ord-173c904036b3494ca7a6e3278b1b792f |
|---|
| 出典メモ | uspto-grants-1997_01 |
|---|
