Cyclopropanemethanamine → 2-Methylpyridine-4-carboxaldehyde(Cyclopropylmethyl)imine

反応式

[CH:1]([C:3]1[CH:8]=[CH:7][N:6]=[C:5]([CH3:9])[CH:4]=1)=O.[CH:10]1([CH2:13][NH2:14])[CH2:12][CH2:11]1>>[CH:10]1([CH2:13][N:14]=[CH:1][C:3]2[CH:8]=[CH:7][N:6]=[C:5]([CH3:9])[CH:4]=2)[CH2:12][CH2:11]1

参加物

反応物 2

HCID 75646Cyclopropanemethanamine

HCID 27630002-METHYLISONICOTINALDEHYDE

生成物 1

HCID 861820892-Methylpyridine-4-carboxaldehyde(Cyclopropylmethyl)imine

実験手順

Reaction of 4-formyl-2-methylpyridine [prepared in Example 33(a)] and cyclopropylmethyl amine by the procedure of example 1(c) affords the title compound as a yellow oil.

出典と根拠

ORDレコード: ord-be7a123627e94091b4d51a1c59808027
出典データセット: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05593991

反応ノート

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