3-Hydroxybenzaldehyde → 3-Isopropoxybenzaldehyde
反応式
[OH:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=[O:6].[CH:10](I)([CH3:12])[CH3:11].C(OC1C=C(CCN)C=CC=1)(C)C>>[CH:10]([O:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=[O:6])([CH3:12])[CH3:11]参加物
4
実験手順
3-Isopropoxybenzaldehyde was prepared from 3-hydroxybenzaldehyde and isopropyl iodide analogous to the procedure described in Example 361. By using the procedure of Example 151 this aldehyde was transformed to 2-(3-isopropoxyphenyl)ethylamine, which was reacted with the product of Example 103, following the procedure of Example 105 to give the titled product.
出典と根拠
- ORDレコード
- ord-e159b6f5e8b74ad6a5b27b503254cc59
- 出典データセット
- uspto-grants-1997_01
- 特許番号
- US05593993
反応ノート
読み込み中…