化工社化工社 化学情報印刷レポート · 研究参考用
Benzoyl Peroxide → Diisobutylene Isopropenylphosphonic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl Peroxide | HCID 7187 | — |
| 反応物 | 2,4,4-Trimethyl-1-pentene | HCID 7868 | — |
| 反応物 | Isopropenylphosphonic acid | HCID 557541 | — |
| 溶媒 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | Diisobutylene Isopropenylphosphonic Acid | HCID 131719388 | — |
反応手順
A high pressure autoclave was charged with 0.11 moles of isopropenylphosphonic acid and 0.132 moles of diisobutylene in ethylene glycol dimethyl ether. The components were reacted for 4 hours at 80° to 82° C. Benzoyl peroxide was used as the polymer initiator. 13C and 31P nuclear magnetic resonance spectra indicated approximately 10 to 30% incorporation of diisobutylene into the polymer reaction product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05594084 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-0a2930ecf82341d0b3c4f1d41f927732 |
| 出典メモ | uspto-grants-1997_01 |