関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-methyl-N-(trimethylsilyl)trifluoroacetamide | HCID 32510 | — |
| 反応物 | Cytosine | HCID 178418229 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 178504300 | HCID 178504300 | — |
反応手順
A bis-trimethylsilylcytosine solution was prepared by suspending 5.78 g of cytosine in 20 ml of dichloromethane and adding 20.57 ml of N-methyl-N-trimethylsilyltrifluoroacetamide in 10 ml of dichloromethane and cooling the resulting solution to 0° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05594124 |
|---|
| 出典データセット | uspto-grants-1997_01 |
|---|
| ORD ID | ord-da6a82f444c049bb8e5c3be1ee440914 |
|---|
| 出典メモ | uspto-grants-1997_01 |
|---|
