化工社化工社 化学情報印刷レポート · 研究参考用
1,1,1,3,3-Pentafluoro-3-methoxy-2-(trifluoromethyl)propane → (CF3)2Chco2H (CF3)2chcf2och3 H2O
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1,1,3,3-Pentafluoro-3-methoxy-2-(trifluoromethyl)propane | HCID 45459 | — |
| 反応物 | 2H-Hexafluoro(2-methylpropanoic acid) | HCID 385606 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | (CF3)2Chco2H (CF3)2chcf2och3 H2O | HCID 131719801 | — |
反応手順
(CF3)2CHCF2OCH3 (ether A, 7.1 g) and a solution of (CF3)2CHCO2H (0.6 g) in water (10 mL) are independently and continuously fed to the reactor over 5 hours. The reactor is preheated to 450° C. and maintained at this temperature throughout the run. The reactor pressure is maintained at about atmospheric pressure. The reactor effluent is scrubbed to remove HF. The product includes CF3CH=CF2 (HFC-1225zc) and HFC-236fa.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05594159 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-beed1cab02414ee8a268d1f5d4d363cc |
| 出典メモ | uspto-grants-1997_01 |