化工社化工社 化学情報印刷レポート · 研究参考用
(3-Methoxyphenyl)boronic acid → N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| 反応物 | N-(5-bromothiophenesulfonyl)pyrrole | HCID 23445587 | — |
| 生成物 | N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole | HCID 22998523 | 93% |
反応手順
N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in 93% yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05594021 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-f4509aa58e704c21a3b7b244031cc66e |
| 出典メモ | uspto-grants-1997_01 |