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Sulfuryl chloride → 2-[(4-Methylphenoxy)methyl]thiophene-3-sulfonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuryl chloride | HCID 24648 | — |
| 反応物 | Sodium hydroxide ethanol | HCID 23692425 | — |
| 反応物 | 2-[(4-Methylphenoxymethyl]thiophene-3-sulfonyl}pyrrole | HCID 86583961 | — |
| 生成物 | 2-[(4-Methylphenoxy)methyl]thiophene-3-sulfonyl chloride | HCID 23445257 | — |
反応手順
2-[(4-methylphenoxy)methyl]thiophene-3-sulfonyl chloride was prepared, as described in Example 64E, using N-{2-[(4-methylphenoxymethyl]thiophene-3-sulfonyl}pyrrole by basic hydrolysis (NaOH/EtOH) followed by conversion to the corresponding sulfonyl chloride, in yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05594021 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-9f5b939a1dc144308375610f33650166 |
| 出典メモ | uspto-grants-1997_01 |