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Phosphate → 2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phosphate | HCID 1061 | — |
| 反応物 | D-1,4-Dithiothreitol | HCID 446094 | — |
| 反応物 | 2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole | HCID 22573078 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol | HCID 22572977 | — |
反応手順
The title compound was prepared according to General Method 14 using 2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole (1.5 g, 4.7 mmol), dithiothreitol (2.9 g, 18.7 mmol), EtOH (50 mL), and phosphate buffer (15 mL). MS (APCI): 296 (M−H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06852711B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-5b61d909b51a46b58d8de41f946ae5e3 |
| 出典メモ | uspto-grants-2005_02 |