HCID 22572976、化合物 → 4-tert-Butyl-5-thiocyanato-benzene-1,2-diamine
反応式
[C:1]([C:5]1[C:6]([S:15][C:16]#[N:17])=[CH:7][C:8]([N+:12]([O-])=O)=[C:9]([NH2:11])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[H][H]>[Ni]>[C:1]([C:5]1[CH:10]=[C:9]([NH2:11])[C:8]([NH2:12])=[CH:7][C:6]=1[S:15][C:16]#[N:17])([CH3:4])([CH3:2])[CH3:3]参加物
4
実験手順
5-tert-Butyl-2-nitro-4-thiocyanato-phenylamine (prepared in Example QQ-2; 3 g, 12 mmol) was hydrogenated using Raney nickel (0.75 g) in the presence of hydrogen as described in General Method 3. MS(APCI): 222(M+H).
出典と根拠
- ORDレコード
- ord-58c3a9b280e84bafba5460fc6f8032f7
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06852711B2
反応ノート
読み込み中…