HCID 13592035、化合物 → 3-(5-Hydroxy-4,6,7-trimethyl-1,3-benzoxathiazol-2-yl)propanol

反応式

C(OC(CCC([O:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][C:21](OCC)=[O:22])[S:16][C:15]=2[C:26]=1[CH3:27])=O)=O)C.C(OC1C(C)=C(C)C2OC(C)SC=2C=1C)(=O)C>>[OH:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][CH2:21][OH:22])[S:16][C:15]=2[C:26]=1[CH3:27]

参加物

反応物 2

HCID 13592035HCID 13592035、化合物

HCID 14802163HCID 14802163、化合物

生成物 1

HCID 1275773-(5-Hydroxy-4,6,7-trimethyl-1,3-benzoxathiazol-2-yl)propanol

実験手順

Ethyl 3-[5-(3-ethoxycarbonylpropionyloxy)-4,6,7-trimethyl-1,3-benzoxathiole-2-yl)propionate (prepared as described in Example 32) was used in the same process as described in (1) above, to give the title compound, whose melting point, infrared absorption spectrum and mass spectrum were the same as those of the product described in (a) above.

出典と根拠

ORDレコード: ord-cc5b225bed534097ab040a37af0f7b85
出典データセット: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04871762

反応ノート

読み込み中…

参加物