化工社化工社 化学情報印刷レポート · 研究参考用
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | Palmitoleic Acid | HCID 445638 | — |
| 反応物 | CID 11268547 | HCID 11268547 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2-Dimethylaminopyridine | HCID 21885 | — |
反応手順
Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 636 mg of palmitoleic acid, 20 ml of dry methylene chloride, 716 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 654 mg of the title compound were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05597846 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-ec2419e8589248568d4d5df51945cc8a |
| 出典メモ | uspto-grants-1997_01 |