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Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | CID 11268547 | HCID 11268547 | — |
| 反応物 | 12-{[(Prop-2-en-1-yloxy)carbonyl]amino}dodecanoic acid | HCID 11652337 | — |
| 溶媒 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 生成物 | 2-Dimethylaminopyridine | HCID 21885 | — |
反応手順
Following a procedure similar to that described in Example 12, but using 547 mg of radicicol, 3.75 g of 12-allyloxycarbonylaminododecanoic acid, 15 ml of dry 1-methyl-2-pyrrolidinone, 1.6 g of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 418 mg of the title compound were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05597846 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-0d49396f87aa4d0694bd0c6068091e57 |
| 出典メモ | uspto-grants-1997_01 |