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Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | 3-Thiophen-2-ylprop-2-enoic acid | HCID 92868 | — |
| 反応物 | CID 11268547 | HCID 11268547 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 2-Dimethylaminopyridine | HCID 21885 | — |
反応手順
Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 462 mg of 3-(2-thienyl)acrylic acid, 10 ml of dry tetrahydrofuran, 619 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 526 mg of the title compound were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05597846 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-fedd808a5f9c4f48b8e6720610baacfd |
| 出典メモ | uspto-grants-1997_01 |