化工社化工社 化学情報印刷レポート · 研究参考用
Lauric Acid → 4-Ethyl-2-undecyl-2-oxazoline-4-methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lauric Acid | HCID 3893 | — |
| 反応物 | 2-Amino-2-ethyl-1,3-propanediol | HCID 8282 | — |
| 生成物 | 4-Ethyl-2-undecyl-2-oxazoline-4-methanol | HCID 91186 | 90.1% |
反応手順
26 g (130 mmoles) of dodecanoic acid and 31 g (260 mmoles) of 2-amino-2-ethyl-1,3-propanediol were condensed together by heating at 185°-190° C. for 30 hours. Work up and distillation of the residue at 160°-162° C./1 mm Hg gave 33.19 g (90%) of the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04876249 |
| 出典データセット | uspto-grants-1989_10 |
| ORD ID | ord-466d60dedc604236b5a36de9f323f12c |
| 出典メモ | uspto-grants-1989_10 |