化工社化工社 化学情報印刷レポート · 研究参考用
Ethylenediamine → 2-(2-Dodecyl)-2-imidazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | 2-Methyldodecanonitrile | HCID 103424 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | 2-(2-Dodecyl)-2-imidazoline | HCID 14651799 | 65% |
反応手順
19.53 g (100 mmoles) of 2-cyanododecane, 8.5ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 15.5 g (65%) of the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04876249 |
| 出典データセット | uspto-grants-1989_10 |
| ORD ID | ord-88eb195044d540eeb46b2c20959d9d81 |
| 出典メモ | uspto-grants-1989_10 |