Ethylenediamine → HCID 14651800、化合物
反応式
[C:1]([C:3]([CH3:13])([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:4])#[N:2].[CH2:14](N)[CH2:15][NH2:16]>C(=S)=S>[CH3:4][C:3]([C:1]1[NH:2][CH2:14][CH2:15][N:16]=1)([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:13]参加物
4
実験手順
18.32 g (100 mmoles) of 2-cyano-2-methyldecane, 8.5 ml (127 mmoles) of ethylenediamine and 0.5 ml of carbon disulfide are reacted according to Example 29 and the reaction mixture is worked up as mentioned therein. Distillation of the residue gives 13.91 g (62%) of the product.
後処理
- distillationDistillation of the residue
出典と根拠
- ORDレコード
- ord-bdba5c0bbe55404592e9833eca563d7c
- 出典データセット
- uspto-grants-1989_10
- 特許番号
- US04876249
反応ノート
読み込み中…