化工社化工社 化学情報印刷レポート · 研究参考用
16-Hydroxyhexadecanoic acid → 2-Dimethylaminopyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 16-Hydroxyhexadecanoic acid | HCID 10466 | — |
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | CID 11268547 | HCID 11268547 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 2-Dimethylaminopyridine | HCID 21885 | — |
反応手順
Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 681 mg of 16-hydroxyhexadecanoic acid, 20 ml of dry tetrahydrofuran, 516 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 661 mg of the title compound were obtained as crystals melting at 85°-86° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05597846 |
| 出典データセット | uspto-grants-1997_01 |
| ORD ID | ord-6cdffb01c49c461caf7871ae4b574e83 |
| 出典メモ | uspto-grants-1997_01 |