1-Methyl-3-aminopyrazole → HCID 23093057、化合物
反応式
CO[C:3](=[O:12])[C:4]1[CH:9]=[C:8](I)[CH:7]=[C:6]([OH:11])[CH:5]=1.[O:13]([CH2:21][C@H:22](O)[CH3:23])[Si](C(C)(C)C)(C)C.[CH3:25][S:26]([C:29]1[CH:34]=[CH:33][C:32]([SH:35])=[CH:31][CH:30]=1)(=[O:28])=[O:27].[NH2:36][C:37]1[CH:41]=[CH:40][N:39]([CH3:42])[N:38]=1>>[OH:13][CH2:21][CH:22]([CH3:23])[O:11][C:6]1[CH:7]=[C:8]([S:35][C:32]2[CH:33]=[CH:34][C:29]([S:26]([CH3:25])(=[O:28])=[O:27])=[CH:30][CH:31]=2)[CH:9]=[C:4]([CH:5]=1)[C:3]([NH:36][C:37]1[CH:41]=[CH:40][N:39]([CH3:42])[N:38]=1)=[O:12]参加物
5
実験手順
The compound of Production Example 133 was obtained as a colorless amorphous substance using 3-hydroxy-5-iodobenzoic acid methyl ester, (2R)-1-(tert-butyldimethylsiloxy)-2-hydroxypropane, 4-methanesulfonylbenzenethiol and 3-amino-1-methyl-1H-pyrazole, by the same method as in Production Example 74 or 82, a corresponding method, or a combination thereof with an ordinary method.