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2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethenylbenzenesulfonamide | HCID 11367403 | — |
| 反応物 | 2,4-Dichloro-6-isocyanato-1,3,5-triazine | HCID 13052624 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide | HCID 20218271 | — |
反応手順
A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04640704 |
| 出典データセット | uspto-grants-1987_02 |
| ORD ID | ord-1df3afabf3e9489b97b7a1acc5d394dd |
| 出典メモ | uspto-grants-1987_02 |