Methane → Choline

HRID 235795

反応式

HRID 235795 の反応式
[OH-:1].[OH:2][CH2:3][CH2:4][N+:5]([CH3:8])([CH3:7])[CH3:6].C>[Cl-].OCC[N+](C)(C)C.O>[OH:2][CH2:3][CH2:4][N+:5]([CH3:8])([CH3:7])[CH3:6].[OH-:1].[OH:2][CH2:3][CH2:4][N+:5]([CH3:8])([CH3:7])[CH3:6]

参加物

6

反応物 2

HCID 297MethaneHCID 31255Choline, hydroxide2 回

生成物 2

HCID 305Choline収率 10%HCID 31255Choline, hydroxide収率 10%

試薬・触媒・溶媒 2

HCID 6209Choline Chloride触媒4 回HCID 962Water溶媒

実験手順

From Choline Chloride and Choline Hydroxide. A 10% choline buffer was prepared from equal portions of 10% choline chloride and 10% choline hydroxide. The 10% choline chloride solution was prepared from 10 g of choline chloride diluted to 100 ml with water. The 10% choline hydroxide solution was prepared by diluting a 50% solution, decolorizing with charcoal, and filtering. Choline hydroxide may also be prepared from choline chloride by ion exchange chromatography.

後処理

  1. filtrationfiltering
  2. customCholine hydroxide may also be prepared from choline chloride by ion exchange chromatography

出典と根拠

ORDレコード
ord-4640fd80830041a09c51ea501b7250fb
出典データセット
uspto-grants-1987_02
特許番号
US04642316

関連ノート

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