関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethyl chloroacetate | HCID 7751 | — |
| 反応物 | Carbonic acid, methyl phenyl ester | HCID 139482 | — |
| 反応物 | Tbpb | HCID 10092649 | — |
| 生成物 | Acetic acid, 2-phenoxy-, ethyl ester | HCID 17365 | 96% |
反応手順
A mixture of 3.8 g of methyl phenyl carbonate, 3.06 g of ethyl chloroacetate, and 0.42 g of TBPB was heated at 120° C. for 2 hours. Distillation of the resulting reaction mixture provided a 96 percent yield of ethyl phenoxyacetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04642349 |
|---|
| 出典データセット | uspto-grants-1987_02 |
|---|
| ORD ID | ord-84617750b2de451891c31139817feac1 |
|---|
| 出典メモ | uspto-grants-1987_02 |
|---|
