化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → (2-Bromophenyl)hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Bromophenylhydrazine hydrochloride | HCID 2723912 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | (2-Bromophenyl)hydrazine | HCID 85583 | — |
反応手順
15 g 2-bromophenylhydrazine hydrochloride are suspended in 400 ml of toluene and combined with 240 ml of 1 N sodium hydroxide solution. The mixture is stirred for 1 hour and the phases are separated. The organic phase is dried on magnesium sulphate and the solvents are eliminated in vacuo. The crude product thus obtained is further reacted directly.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08686022B2 |
| 出典データセット | uspto-grants-2014_04 |
| ORD ID | ord-15172afbc4084c749fa1d4454ea24d19 |
| 出典メモ | uspto-grants-2014_04 |