化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 8-Hydroxy-2-methyl-7-quinolinecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 8-Hydroxy-2-methyl-7-quinolinecarboxylic acid methyl ester | HCID 54511211 | — |
| 生成物 | 8-Hydroxy-2-methyl-7-quinolinecarboxamide | HCID 21271472 | — |
反応手順
8-Hydroxy-2-methyl-7-quinolinecarboxylic acid methyl ester is reacted with excess ammonia in a steel bomb for 12-18 hr. The excess ammonia is allowed to evaporate and the residue is crystallized from a suitable solvent to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04642343 |
| 出典データセット | uspto-grants-1987_02 |
| ORD ID | ord-833cdc1c912c44cfbecbe45644db9f04 |
| 出典メモ | uspto-grants-1987_02 |