Hydrochloric Acid → Diisopropylamino-acetic acid hydrochloride

HRID 2364929ノート

反応式

HRID 2364929 の反応式
C([O:5][C:6](=[O:15])[CH2:7][N:8]([CH:12]([CH3:14])[CH3:13])[CH:9]([CH3:11])[CH3:10])(C)(C)C.[ClH:16]>O>[ClH:16].[CH:9]([N:8]([CH2:7][C:6]([OH:15])=[O:5])[CH:12]([CH3:13])[CH3:14])([CH3:10])[CH3:11]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 11333389HCID 11333389、化合物

生成物 1

HCID 46735981Diisopropylamino-acetic acid hydrochloride

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

5.4 g (25 mMol) diisopropylamino-acetic acid tert-butylester 2 was stirred with 6.25 ml (75 mMol) 12 M HCl in 25 ml water for 2.5 h at 60° C. After distillation in vacuo of water and excess of HCl, the residue was dried with toluene azeotropically.

後処理

  1. distillationAfter distillation in vacuo of water
  2. dry with materialexcess of HCl, the residue was dried with toluene azeotropically

出典と根拠

ORDレコード
ord-ebb2f625df644252aacb55878745cfe1
出典データセット
uspto-grants-2014_04
特許番号
US08697604B2

反応ノート

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