化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 178512607、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Bromo-2'-nitroacetophenone | HCID 244025 | — |
| 反応物 | HCID 178513045 | HCID 178513045 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 178512607 | HCID 178512607 | 95% |
反応手順
A solution of 16.5 gm of 2-nitro-phenacyl bromide and 7.98 gm of amidinothiourea in 70 ml of dimethylformamide was stirred at room temperature for 16 hours, and then poured into 350 ml of water. The solution was made alkaline with 10% sodium hydroxide, and the solid which separated out after cooling was filtered, washed with water and dried, yielding 16.9 gm of the title compound, m.p. 176°-178° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04645841 |
| 出典データセット | uspto-grants-1987_02 |
| ORD ID | ord-0999f81bbcdc4f8fac59951338ee04e7 |
| 出典メモ | uspto-grants-1987_02 |