化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Acetate → Ethyl 2-[(acetyloxy)methyl]oxazole-4-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Acetate | HCID 517044 | — |
| 反応物 | Ethyl 2-(bromomethyl)-1,3-oxazole-4-carboxylate | HCID 641223 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | Ethyl 2-[(acetyloxy)methyl]oxazole-4-carboxylate | HCID 67280692 | — |
反応手順
9.5 g (10.80 mmol) of ethyl 2-(bromomethyl)oxazole-4-carboxylate are dissolved in 135 mL of acetonitrile. 9.96 g (101.47 mmol) of potassium acetate are added and the medium is stirred at room temperature for 14 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08697883B2 |
| 出典データセット | uspto-grants-2014_04 |
| ORD ID | ord-6cfbc40eae4848079a2eea988c375067 |
| 出典メモ | uspto-grants-2014_04 |