化工社化工社 化学情報印刷レポート · 研究参考用
Tetraethylenepentamine → Sodium orthosilicate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetraethylenepentamine | HCID 8197 | — |
| 反応物 | Crotyl chloride | HCID 11589 | — |
| 反応物 | Sodium silicate pentahydrate | HCID 86733098 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium orthosilicate | HCID 26051 | — |
反応手順
One mol of sodium silicate pentahydrate, one mol of methyl allyl chloride, one mol of tetraethylenepentamine and 300% by weight of water, percentage based on weight of the reactants, are mixed; 1.5 mols of dihalohydrin are slowly added while agitating and keeping the temperature below 70° C. for 10 to 60 minutes thereby producing a water soluble resinous product and sodium silicate. This aqueous solution may be diluted with water and used as an adhesive and to improve wet strangth. The paper is cured by heating the paper to 80° to 120° C. for 10 to 60 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04157438 |
| 出典データセット | uspto-grants-1979_06 |
| ORD ID | ord-02fe06a9b0354ad78687d9417d9f67f0 |
| 出典メモ | uspto-grants-1979_06 |