HCID 46947540、化合物 → HCID 46947721、化合物

HRID 2370589ノート

反応式

HRID 2370589 の反応式
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCCCC(F)(F)[F:64])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:43][C:2]1([CH3:1])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:64])[F:26])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:40])([F:41])[F:39])[CH:30]=2)[C:3]1=[O:42]

参加物

3

反応物 2

HCID 46947540HCID 46947540、化合物HCID 46947720HCID 46947720、化合物

生成物 1

HCID 46947721HCID 46947721、化合物収率 73%

実験手順

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 12 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 73% (140 mg).

後処理

  1. customA pale yellow oil is obtained with a yield of 73% (140 mg)

出典と根拠

ORDレコード
ord-350ac0f647b44297a99ff8f16af2025d
出典データセット
uspto-grants-2014_04
特許番号
US08710091B2

反応ノート

読み込み中…