HCID 46944971、化合物 → HCID 46944972、化合物

HRID 2370590ノート

反応式

HRID 2370590 の反応式
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19]CC(F)(F)C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCC[C:62]([F:74])([F:73])[C:63]([F:72])([F:71])[C:64]([F:70])([F:69])[C:65]([F:68])([F:67])[F:66])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][C:62]([F:74])([F:73])[C:63]([F:71])([F:72])[C:64]([F:69])([F:70])[C:65]([F:68])([F:67])[F:66])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:39])([F:41])[F:40])[CH:30]=2)[C:3]1=[O:42]

参加物

3

反応物 2

HCID 46944971HCID 46944971、化合物HCID 46947540HCID 46947540、化合物

生成物 1

HCID 46944972HCID 46944972、化合物収率 85%

実験手順

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 14 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 85% (145 mg).

後処理

  1. customA pale yellow oil is obtained with a yield of 85% (145 mg)

出典と根拠

ORDレコード
ord-91463e120e5b486687652ee19ef089a5
出典データセット
uspto-grants-2014_04
特許番号
US08710091B2

反応ノート

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