HCID 46945366、化合物 → HCID 46945557、化合物

HRID 2370598ノート

反応式

HRID 2370598 の反応式
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])[C:22]([F:25])([F:24])[F:23])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-])=O)=[C:31]([C:38](F)(F)F)[CH:30]=2)[C:3]1=[O:42].NC1C=[CH:49][C:48]([N:51]2C(=O)C(C)(C)N(CCCCCCCCCSCCCC(F)(F)C(F)(F)F)[C:52]2=[O:79])=[CH:47][C:46]=1C>>[CH3:1][C:2]1([CH3:43])[C:3](=[O:42])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([NH:35][C:52]([NH:51][CH:48]([CH3:49])[CH2:47][CH3:46])=[O:79])=[C:31]([CH3:38])[CH:30]=2)[C:5](=[O:28])[N:6]1[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][CH2:20][C:21]([F:27])([F:26])[C:22]([F:23])([F:25])[F:24])=[O:17]

参加物

3

反応物 2

HCID 46945366HCID 46945366、化合物HCID 46947540HCID 46947540、化合物

生成物 1

HCID 46945557HCID 46945557、化合物収率 63%

実験手順

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 25 replacing the compound of Example 1. A colourless oil is obtained with a yield of 63%.

後処理

  1. customA colourless oil is obtained with a yield of 63%

出典と根拠

ORDレコード
ord-b4ac3c9c6dc544e99066d0aef92eeb44
出典データセット
uspto-grants-2014_04
特許番号
US08710091B2

反応ノート

読み込み中…