Hydrochloric Acid → (R)-3-Allylsulfanyl-2-amino-propionic acid methyl ester hydrochloride
反応式
[CH3:1][O:2][C:3](=[O:18])[C@@H:4]([NH:10]C(OC(C)(C)C)=O)[CH2:5][S:6][CH2:7][CH:8]=[CH2:9].[ClH:19]>O1CCOCC1>[ClH:19].[CH3:1][O:2][C:3](=[O:18])[C@@H:4]([NH2:10])[CH2:5][S:6][CH2:7][CH:8]=[CH2:9]参加物
4
実験手順
Methyl ester 29 (3.20 g, 11.6 mmol) was dissolved in 4M hydrogen chloride in 1,4-dioxane (40 mL). The resultant solution was stirred at rt for 18 h before being concentrated in vacuo to yield a white solid, 2.46 g, 100%.
後処理
- concentrationbefore being concentrated in vacuo
- customto yield a white solid, 2.46 g, 100%
出典と根拠
- ORDレコード
- ord-d7a93993265f436cb5f9f87213894c36
- 出典データセット
- uspto-grants-2014_04
- 特許番号
- US08710178B2
反応ノート
読み込み中…