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4-Bromophenacyl bromide → tert-butyl N-[2-(4-bromophenyl)-2-hydroxyethyl]-N-methylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Bromophenacyl bromide | HCID 7454 | — |
| 反応物 | tert-Butyl 2-hydroxy-2-(4-morpholin-4-ylphenyl)ethyl(methyl)carbamate | HCID 22574361 | — |
| 生成物 | tert-butyl N-[2-(4-bromophenyl)-2-hydroxyethyl]-N-methylcarbamate | HCID 22574334 | — |
反応手順
As described for the preparation of tert-Butyl 2-hydroxy-2-(4-morpholin-4-ylphenyl)ethyl(methyl)carbamate (Preparations 87-88), 2,4′-dibromoacetophenone was converted to the title compound, isolated as a pale yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06852731B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-8e56bd0d17494d0eadb3bf291f1a949e |
| 出典メモ | uspto-grants-2005_02 |