化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → 3-Phenylammonio-1-propanesulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Propane sultone | HCID 14264 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 3-Phenylammonio-1-propanesulfonate | HCID 12546060 | 95% |
反応手順
A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642014B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-f03ab8001ee74a3fa69d20bb82c32bc4 |
| 出典メモ | uspto-grants-2014_02 |