化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Chloride → HCID 178446842、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Chloride | HCID 5234 | — |
| 反応物 | 2-[4-(Aminomethyl)phenyl]benzonitrile | HCID 1393341 | — |
| 反応物 | Methyl valerimidate hydrochloride | HCID 5743465 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 178446842 | HCID 178446842 | — |
反応手順
The title compound is prepared by stirring one equivalent of methyl valerimidate hydrochloride, one equivalent of 4-aminomethyl-2'-cyanobiphenyl, and one equivalent of sodium methoxide in methanol. The reaction mixture may then be stripped of solvent and the amidine and residual sodium chloride is used directly in the next reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05100897 |
| 出典データセット | uspto-grants-1992_03 |
| ORD ID | ord-5a45ac59856143d1af6da106ced1c6e8 |
| 出典メモ | uspto-grants-1992_03 |