化工社化工社 化学情報印刷レポート · 研究参考用
3-Cyanophenol → O-3-cyanophenyl dimethylthiocarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Cyanophenol | HCID 13394 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| 生成物 | O-3-cyanophenyl dimethylthiocarbamate | HCID 14795402 | — |
反応手順
If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05101048 |
| 出典データセット | uspto-grants-1992_03 |
| ORD ID | ord-87ff7015c4e34deb8be2f93ca8168df5 |
| 出典メモ | uspto-grants-1992_03 |