化工社化工社 化学情報印刷レポート · 研究参考用
Sodium methanethiolate → 3,5-Dicyano-2-mercaptobenzonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium methanethiolate | HCID 4378561 | — |
| 反応物 | 2-Bromobenzene-1,3,5-tricarbonitrile | HCID 12575939 | — |
| 生成物 | 3,5-Dicyano-2-mercaptobenzonitrile | HCID 14795337 | — |
反応手順
If the procedure described in Preparation LV is followed starting from 6 g (26.10-3 mol) of 2-bromo-3,5-dicyanobenzonitrile and 6 g (86.10-3 mol) of sodium thiomethylate, 6 g (quantitative yield) of the expected product are obtained in the form of an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05101048 |
| 出典データセット | uspto-grants-1992_03 |
| ORD ID | ord-0be296470203476582048edd0b81c4af |
| 出典メモ | uspto-grants-1992_03 |