Furan, 2-(bromomethyl)tetrahydro- → 2-((4-Bromo-3,5-dimethylphenoxy)methyl)tetrahydrofuran
反応式
[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([OH:9])=[CH:4][C:3]=1[CH3:10].Br[CH2:12][CH:13]1[CH2:17][CH2:16][CH2:15][O:14]1>>[Br:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([O:9][CH2:12][CH:13]2[CH2:17][CH2:16][CH2:15][O:14]2)=[CH:4][C:3]=1[CH3:10]参加物
3
実験手順
The title compound is prepared from 4-bromo-3,5-dimethylphenol and 2-(bromomethyl)tetrahydrofuran following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 1): tR=1.37 min; Mass spectrum (ESI+): m/z=285 [M+H]+.
出典と根拠
- ORDレコード
- ord-ee837e2e06dd4b118cf671e3ba95d661
- 出典データセット
- uspto-grants-2014_02
- 特許番号
- US08642585B2
反応ノート
読み込み中…