化工社化工社 化学情報印刷レポート · 研究参考用
2H-1,4-benzoxazin-3(4H)-one → 6-(6-Bromohexanoyl)-2H-1,4-benzoxazin-3(4H)-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2H-1,4-benzoxazin-3(4H)-one | HCID 72757 | — |
| 反応物 | 6-Bromohexanoyl chloride | HCID 89848 | — |
| 生成物 | 6-(6-Bromohexanoyl)-2H-1,4-benzoxazin-3(4H)-one | HCID 21886993 | — |
反応手順
Using 2H-1,4-benzoxazin-3(4H)-one (15.0 g) and 6-bromohexanoyl chloride (2.5.8 g) according to the same method as that of Reference Example 1, the title compound (14.8 g) was obtained as colorless crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07462628B2 |
| 出典データセット | uspto-grants-2008_12 |
| ORD ID | ord-fd0ce46667bb4f2cbc3d72676cd96cd6 |
| 出典メモ | uspto-grants-2008_12 |