関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 4-Bromopyridazine hydrobromide | HCID 53407906 | — |
| 反応物 | 2,6-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline | HCID 56737724 | — |
| 生成物 | 2,6-Dimethyl-4-(pyridazin-4-yl)aniline | HCID 86697255 | — |
反応手順
The title compound is prepared from 4-bromopyridazine hydrobromide and 2,6-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline following a procedure analogous to that described in Step 2 of Intermediate 62. The mixture is stirred for 12 hours at 70° C. LC (method 9): tR=0.66 min; Mass spectrum (ESI+): m/z=200 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08642585B2 |
|---|
| 出典データセット | uspto-grants-2014_02 |
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| ORD ID | ord-7d7e54162d134245a1342a2d2b21f54c |
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| 出典メモ | uspto-grants-2014_02 |
|---|
