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2-Iodo-1-methyl-1H-imidazole → 2-(4-Chloro-3,5-dimethyl-phenyl)-1-methyl-imidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Iodo-1-methyl-1H-imidazole | HCID 335835 | — |
| 反応物 | 2-(4-Chloro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 53217128 | — |
| 生成物 | 2-(4-Chloro-3,5-dimethyl-phenyl)-1-methyl-imidazole | HCID 86697359 | — |
反応手順
The title compound is prepared from 2-chloro-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 2-iodo-1-methyl-imidazole following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 7): tR=0.80 min; Mass spectrum (ESI+): m/z=221/223 (Cl) [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642585B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-44ad746cb51945db9391ac7c5e9924e1 |
| 出典メモ | uspto-grants-2014_02 |