3,5-Dichloro-2-hydroxybenzenesulphonyl chloride → 3-(3,5-Dichloro-2-hydroxybenzenesulfonamido)-2-(2,4-dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)propan-2-ol

HRID 2379101ノート

反応式

HRID 2379101 の反応式
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]([OH:18])([CH2:16][NH2:17])[CH2:10][N:11]1[CH:15]=[N:14][CH:13]=[N:12]1.[Cl:19][C:20]1[C:21]([OH:31])=[C:22]([S:27](Cl)(=[O:29])=[O:28])[CH:23]=[C:24]([Cl:26])[CH:25]=1>>[Cl:19][C:20]1[C:21]([OH:31])=[C:22]([S:27]([NH:17][CH2:16][C:9]([C:3]2[CH:4]=[CH:5][C:6]([Cl:8])=[CH:7][C:2]=2[Cl:1])([OH:18])[CH2:10][N:11]2[CH:15]=[N:14][CH:13]=[N:12]2)(=[O:29])=[O:28])[CH:23]=[C:24]([Cl:26])[CH:25]=1

参加物

3

反応物 2

HCID 900783,5-Dichloro-2-hydroxybenzenesulphonyl chlorideHCID 147065211-[3-Amino-2-(2,4-dichlorophenyl)-2-hydroxyprop-1-yl]-1H-1,2,4-triazole

生成物 1

HCID 189579723-(3,5-Dichloro-2-hydroxybenzenesulfonamido)-2-(2,4-dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)propan-2-ol

実験手順

Following the procedure described in the preceeding examples but using 2-(2,4-dichlorophenyl)-3-amino-1-(1H-1,2,4-triazol-1-yl)propan-2-ol and 3,5-dichloro-2-hydroxybenzenesulfonylchloride, the title compound was obtained in a similar yield:

出典と根拠

ORDレコード
ord-517d31ebe11441b0945dd89076763711
出典データセット
uspto-grants-1994_11
特許番号
US05360813

反応ノート

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